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1 article(s) from Kleij, Arjan W

Comparing kinetic profiles between bifunctional and binary type of Zn(salen)-based catalysts for organic carbonate formation

Carmen Martín and
Arjan W. Kleij

Beilstein J. Org. Chem. 2014, 10, 1817–1825, doi:10.3762/bjoc.10.191

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Scheme 1: Catalytic synthesis of organic (poly)carbonates from epoxides and CO₂.

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Figure 1: Structures of some metal complexes used as catalyst for (cyclic) organic carbonate synthesis.

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Scheme 2: Proposed mechanistic cycle for cyclic carbonate synthesis mediated by Zn(salphen) complexes in the ...

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Figure 2: Typical ¹H NMR spectrum of a sample of a crude mixture in CDCl₃ (300 MHz) at rt.

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Scheme 3: Proposed mechanism for the formation of cyclic carbonates mediated by an ammonium salt.

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Figure 3: Double logarithmic plot and to determinate the order in NBu₄I. Conditions: 1,2-epoxyhexane (10 mmol...

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Figure 4: Double logarithmic plot to determine the order in binary catalyst Zn(salphen) 1/NBu₄I in the presen...

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Figure 5: Double logarithmic plot to determine the order in binary catalyst Zn(salphen) 1/NBu₄I in the presen...

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Figure 6: Double logarithmic plot to determine the order with respect to the binary system NBu₄I/Zn complex 1...

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Figure 7: Proposed association for complex 2 and schematic structure for bifunctional complex 9.

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Figure 8: Double logarithmic plot to determine the order in Zn complex 2. Conditions: 1,2-epoxyhexane (10 mmo...

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Scheme 4: On the left a dimetallic mechanism proposed for bifunctional catalyst 2 and on the right a monometa...

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Figure 9: Double logarithmic plot to determine the order with respect to the bifunctional Zn complex 2 in the...

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Published 08 Aug 2014

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